Analytical

AUTO TITRATOR TITRA SMART

Titration is the fundamental chemical analysis procedure whereby concentration of chemical substance in solution is determined by reacting it with measured amount of another chemical. Auto titrator performs this analysis using motor driven dispenser, stirred reaction vessel and electrodes which sense the completion of reaction by measuring the potential difference between two electrodes. Making use of this instrument, it is possible to increase the accuracy, repeatability, reproducibility and minimize the errors in calculation and documentation.

The instrument provides following modes of Titrations :

- Incremental :

Incremental titration operates with user selectable fixed dose and fixed intervals till the end point is detected or volume limit is reached.

-Equilibrium :

This is universal and dynamic titration. In this titration the dose and time automatically get tuned to the titration trend with evaluation of end point.

The following Titrations are possible with TITRA

  • Acid-base or aqueous titration
  • Nonaqueous titration
  • Redox titration
  • Argentometric or Precipitation titration
  • Complexometric titration or EDTA titration
  • Voltametric titration / KF Titration
  • Blank titration
  • Back titration
  • Silver Assay Titrations (As per BIS 2113 : 2002)

Applications

  • Pharmaceuticals and Bio-Chemistry
  • Environmental and Water Pollution
  • Food and Beverages
  • Dyes and Chemicals
  • Pesticides and Fertilizers
  • Petrochemicals, Plastics and Polymers
  • Metallurgy and Electroplating
  • Jewellery Industry

 

TITRA SMART is provided with two-point auto calibration and standardisation (zero offset). The instrument is capable of displaying pH and mV of the sample, with temperature compensation. TITRA SMART can accept a variety of electrodes to cater to various applications in different fields. The liquid path comprises Teflon tubings,Teflon lined valve and gas tight burette with Teflon plunger head. It creates chemically inert system for any sensitive analysis. The instrument is supplied with high speed vortex stirrer with digital speed indication. This specially designed stirrer provides excellent homogenous mixing of samples. An optional magnetic stirrer is also available.

 

Featrues:

User interactive for ease of operation with protection against invalid entries.

Vortex stirrer for vigorous and homogenous stirring with specially designed glass propeller for total chemical inertness.

Quick interchangeable imported burette assemblies with intelligent recognition for its volume size. Burette factor for dispensing corrections is available for true end point calculations.

System recognises proper connectivity of other peripherals like Burette, Stirrer, Electrode etc. gives indication incase of improper connectivity.

Composite Differential Electrode Amplifier unit for Potentiometric and Voltametric / KF Titrations, having connectivity to various Electrodes. Temperature Sensor with 4-line measurement technique ensures correct temperature indication. 

Large memory capacity for method storage with suitable scientific parameters having GLP compliance.

Standardised modes of titration, namely incremental, equilibrium of titration.

By selecting titration method, instrument prints the type of appropriate electrode.

During titration, the measured variable i.e. electrode potential (mV) or the pH value is shown on the display together with dispensed volume and number of End Points (EP) detected.

User selectable End Point (EP) evaluation up to 9 EP during the run, and calculation by first, last, largest, all or selected EP with display of results and printout.

Sample Name, Titrant Name, Identification Number, Date with type of Electrode used for authentication. Daily Auto Incremented Run number and Factory entered CUSTOMER NAME and Instrument Sr. No. on report printouts make the system foolproof and GLP compliant.

Facility to use as a dispenser for fixed volume dosing or dilution allows to perform manual titration with user defined dose and mV indication.

Predispense facility with selectable dose and time for quick titrant addition without disturbing the titration trend.

Automatic evaluation of molarity for standardisation of titrant, storage of 20 molarities and their retrieval for calculation.

Compliant to ASTM D664, D2896 & D4739 for TAN and TBN analysis for oil samples.

Titrant temperature factor for volume correction.

Result recalculation facility to obtain printout in different units such as molarity, factor, % assay (wt), % volume (ml), ppm, mg/l, mg/g, ml/g, g/l, meq/l, mol/kg, TAN & TBN for oil samples.

User-defined formula by using constant codes FC 1, FC 2, FC 3, FC 4

Reprocessing of threshold and recalculation of EP without performing the new run.

Statistic function with Run Selectivity for finding Mean, S.D., R.S.D., and C.V. of last 10 repeat run results could be viewed or printed.

User Programmed selectivity for report format, complying with GLP requirements:

a) Report giving parameter and result.

b) Data table giving mV, pH, mV, mV/ml, 2nd derivative and volume (μl).

c) Graphics report giving mV v/s μl titration curve.

d) Graphics report 1st derivative graph v/s μl titration curve.

e) Graphical report of 2 derivative curve.

f) Report of method parameters for 50 methods.

g) Condensed report of titration parameters and results.

h) Auto evaluation report for multi EP samples - EP1, EP2-EP1 etc. available.

The reports can be obtained even after resetting/power off/power fail conditions.

  • Time display and report printout with run time indication.
  • Balance interface to directly transfer the sample weight.
  • TITRA can be conver ted to perform Karl Fischer titrations by simply changing burette assembly. All the specifications of LABINDIA Karl Fischer Titrator are applicable.
  • Online graphic display to analyse Sample Reaction Trend.
  • Display Syringe filled status on screen.

 

Specifications:

Principle : Volume determination by equivalence point, end point.

mV range : ±3200 mV.

Accuracy : ±0.1 mV (±0.0016 pH)

Polarized Sensor Measurement range: 0 to ±3200 mV / 0 to ±80 μA

Polarized Sensor Resolution: 0.1 mV / 0.1 μA

Amplifier input impedance : > 10-12 ohms

Burette Resolution : 1/5000 for 5 ml (i.e. 1 microlitre), 1/10000 for 10 ml (i.e. 1 microlitre), 1/5000 for 5 ml (i.e. 5 microlitre)

Filling time : <20 sec.

Keyboard : Qwerty Keyboard.

Display : 7thTOUCH SCREEN

Titration Head : (a) Manual stand with swivelling arm.

Stirrer System : Microcontroller based variable speed, high torque vortex stirrer with digital indication. Magnetic Stirrer optional.

Sensors :

(1) Electrodes for Potentiometric titration - (pH, Ion, Redox, Argentometric, Non-Aqueous & Complexometric).

a) Any combination electrode.

b) Differential Electrode System comprising sensing (Indicator) Electrode with BNC Connector and Reference Electrode with 4mm Banana Connector.

(2) Electrode for KF / Voltametric titration with BNC/TNC Connectors.

(3) Temperature sensor (PRT/PT100)

Calibration : 3-point Calibration with user entered buffer values and standardisation with 7 pH buffer.

End Point detection : a) Potentiometric b) Voltametric

Cut-off criteria : a) Volume b) End point c) mV/pH.

Methods :

1) Titrations - a) Acid base, b) Non-aqueous. c) Redox d) Preciptiation e) Complexometric f) back titration

2) KF titration (Optional)

Results : a) Molarity b) % Assay (wt) c) % volume (ml) d) ppm e) mg/l f) mg/g g) g/l h) meq/l i) mol/kg j) TAN and TBN for oil samples.

Method Storage : 16 GB data storage capacity for 200 methods and results.

Titrant Molarity storage : 20 values

Report Format : 1) Method Parameters 2) Titration analysis report 3) Titration analysis condensed report 4) Titration data table

5) Titration graphic report - i) μl v/s mV ii) μl v/s First derivative iii) μl v/s Second derivative iv) μl v/s Time

6) Auto evaluation report 7) Statistics report 8) End Point Titration report 9) Calibration report.

Input/Output Peripheral Interface : (a) Serial Port: 1 Nos. - for Balance (b) USB Connectivity for data backup, software upgradation and printer connectivity

(c) Laserjet printer connectivity through wireless LAN

Power : 230 V AC ± 10%, 50 Hz.

Environmental Operating Conditions : a) Operation : Indoor b) Temperature : Ambient to 45°C c) Humidity : 5 to 90% non-condensing.

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